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The response tolerated An array of practical groups and bring on the corresponding products in reasonable to excellent yields.
oxidation of reagent 7a to azodicarboxylate 2a (see also Plan 5). Nevertheless, C–N bond formation with hydrazine dicarboxylate 7a within the Chan–Evans–Lam response can't be excluded.21
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Correct mass figures with the protonated molecular and predominant product ions, and their proposed chemical formulae acquired for compounds 1–5 calculated by liquid chromatography–large-resolution mass spectrometry (/mass spectrometry)
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Even though the reaction of meta- or para-nitro-substituted acetophenone oxime derivatives was successfully performed to afford average to excellent yields of preferred products, the two-nitrobenzaldehyde oxime methyl ether only gave the corresponding indazole 36 inside a average produce on Contact Here account of steric results within the aryl ring. The unsubstituted acetophenone oxime derivatives were all well suited for This technique, resulting in ideal indazoles in satisfactory yields. In the following move, equally p
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